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Solid / Soil Matrix2
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Analyte |
Method |
Sample Quantity1,2
|
Container Type |
Preservation |
Hold Time |
|
WetChemistry |
|
|
|
|
Chloride |
SW846 9251 or 9056 |
50 g |
plastic or glass |
none |
28 days |
|
Corrosivity (pH only) |
SW846 9045D |
50 g |
plastic or glass |
none |
immediately |
|
Cyanide-Amenable |
SW846 9013 |
20 g |
plastic or glass |
cool 4oC |
14 days |
|
Cyanide-Total |
SW846 9012B |
20 g |
plastic or glass |
cool 4oC |
14 days |
|
Flash Point |
SW846 1010A |
30 g |
plastic or glass |
cool 4oC |
NA |
|
Fluoride |
SW846 9214 or 9056 |
20 g |
plastic or glass |
cool 4oC |
28 days |
|
Free Liquids |
SW846 9095B |
200 g |
plastic or glass |
none |
NA |
|
Grain Size (Sieve) |
ASTM 2488-84 |
500 g |
plastic or glass |
none |
NA |
|
Ignitability |
SW846 1010A |
30 g |
plastic or glass |
cool 4oC |
NA |
|
Oil & Grease (Hexane) |
EPA 1664A Mod. |
60 g |
plastic or glass |
cool 4oC |
28 days |
|
Oil & Grease (Hexane/SGT) (TRPH) |
EPA 1664A Mod. |
60 g |
plastic or glass |
cool 4oC |
28 days |
|
pH |
SW846 9045D |
50 g |
plastic or glass |
none |
immediately |
|
Phenolics |
SW846 9066 |
30 g |
plastic or glass |
cool 4oC |
28 days |
|
Phosphate-Total |
EPA 365.1 Mod. |
30 g |
plastic or glass |
cool 4oC |
28 days |
|
Reactive Cyanide |
SW846 Vol 1C Chap. 7, 8.3/7.3.3 |
30 g |
plastic or glass |
cool 4oC |
7 days |
|
Reactive Sulfide |
SW846 Vol 1C Chap. 7, 8.3/7.3.4 |
30 g |
plastic or glass |
cool 4oC |
7 days |
|
Solids-Fixed |
SM2540G |
20 g |
plastic or glass |
cool 4oC |
7 days |
|
Solids-Total |
SM2540B&G |
20 g |
plastic or glass |
cool 4oC |
7 days |
|
Solids-Volatile |
EPA 160.4 & SM2510G |
20 g |
plastic or glass |
cool 4oC |
7 days |
|
Sulfate |
SW846 9038 or 9056 |
50 g |
plastic or glass |
cool 4oC |
28 days |
|
Total Organic Carbon (TOC) |
SW846 9060 (not performed at AWAL) |
20 g |
plastic or glass |
cool 4oC |
28 days |
|
Total Organic Halides (TOX) |
SW846 9020B |
20 g |
plastic or glass |
cool 4oC |
28 days |
|
Total Recoverable Petroleum
Hydrocarbons |
EPA 1664A Modified |
60 g |
plastic or glass |
cool 4oC |
28 days |
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1 - This does not include the volume necessary to perform MS/MSD analyses. Include additional sample (normally 3 times the quoted volume or mass) for each sample requiring an MS/MSD. This extra sample volume should always be included for at least one sample in sample sets of 5 or greater. Contact the laboratory for more information. |
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2 - For reporting results in dry weight a total solid analysis must be included. Be sure to collect a sample for total solids. |